dc.contributor.author | Adilina, Indri Badria | |
dc.contributor.author | Tasrif | |
dc.contributor.author | Laksmono, Joddy Arya | |
dc.contributor.author | Agustian, Egi | |
dc.date.accessioned | 2010-10-06T02:29:39Z | |
dc.date.available | 2010-10-06T02:29:39Z | |
dc.date.issued | 2005 | |
dc.identifier.uri | http://repository.ipb.ac.id/handle/123456789/40478 | |
dc.description.abstract | Synthesis of menthol (CWH100) from citronellal (CIIH",O) has been performed by a one-pot process. The process was conducted in a 250 mL capacity auloe/al'e wilh acidified nalural =eolite and Raney Nickel as catalYSIS at temperature 120°e. pressure 5 bar, and varialion of time 1-8 hours. Natural =eolite and Raney Nickel were placed in the aUloc/aI'e and it was found Ihat Ihe cye/isalion and hydrogenation reaclion 10 form menthol could undergo in the same reactor. FTJR Analysis showed peak formation at 3346.50 cm-' indicating OH group was formed Result of I H-NMR and /3C-NMR analysis reports chemical shifts at 6= 71. 53 ppm and ,)=4.05 ppm. Gas chromatography analysis showed thaI the com'ersiol1 was 80% with concentration ofmenthol about 68% (v/v). | id |
dc.publisher | IPB (Bogor Agricultural University) | |
dc.relation.ispartofseries | Vol. 17 No.3 | |
dc.title | One-pot syntesis of menthol from citronellal: application of citronellal: application of citronella oil | id |
dc.title.alternative | Jurnal Teknologi Industri Pertanian Vol 17(3) | |