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Title: | One-pot syntesis of menthol from citronellal: application of citronellal: application of citronella oil |
Other Titles: | Jurnal Teknologi Industri Pertanian Vol 17(3) |
Authors: | Adilina, Indri Badria Tasrif Laksmono, Joddy Arya Agustian, Egi |
Issue Date: | 2005 |
Publisher: | IPB (Bogor Agricultural University) |
Series/Report no.: | Vol. 17 No.3 |
Abstract: | Synthesis of menthol (CWH100) from citronellal (CIIH",O) has been performed by a one-pot process. The process was conducted in a 250 mL capacity auloe/al'e wilh acidified nalural =eolite and Raney Nickel as catalYSIS at temperature 120°e. pressure 5 bar, and varialion of time 1-8 hours. Natural =eolite and Raney Nickel were placed in the aUloc/aI'e and it was found Ihat Ihe cye/isalion and hydrogenation reaclion 10 form menthol could undergo in the same reactor. FTJR Analysis showed peak formation at 3346.50 cm-' indicating OH group was formed Result of I H-NMR and /3C-NMR analysis reports chemical shifts at 6= 71. 53 ppm and ,)=4.05 ppm. Gas chromatography analysis showed thaI the com'ersiol1 was 80% with concentration ofmenthol about 68% (v/v). |
URI: | http://repository.ipb.ac.id/handle/123456789/40478 |
Appears in Collections: | Jurnal Teknologi Industri Pertanian |
Files in This Item:
File | Description | Size | Format | |
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One-Pot Syntesis Of Menthol From Citronellal.pdf | Jurnal | 353.84 kB | Adobe PDF | ![]() View/Open |
One-Pot Syntesis Of Menthol From Citronellal_abstract.pdf | Abstract | 117.94 kB | Adobe PDF | ![]() View/Open |
One-Pot Syntesis Of Menthol From Citronellal_abstract.ps | PostScript | 240.83 kB | Postscript | View/Open |
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